First operation; deoxidization of the ore, and fusion of the tin
A Dictionary of Arts, Manufactures and Mines · 1840 · p. 1267
—Before throwing the ore into the smelting furnace, it is mixed with from one-fifth to one-eighth of its weight of blind coal , in powder, called culm ; and a little slaked lime is sometimes added, to render the ore more fusible. These matters are carefully blended, and damped with water, to render the charging easier, and to prevent the blast from sweeping any of it away at the commencement. From 12 to 16 cwt. are introduced at a charge; and the doors are immediately closed and luted, while the heat is progre ively raised. Were the fire too strong at first, the tin oxide would unite with the quartz of the gangue, and form an enamel. The heat is applied for 6 or 8 hours, during which the doors are not opened; of course the materials are not stirred. By this time the reduction is, in general, finished; the door of the furnace is removed, and the melted ma is worked up to complete the separation of the tin from the scoriæ, and to ascertain if the operation be in sufficient forwardne . When the reduction seems to be finished, the scoriæ are taken out at the same door, with an iron rake, and divided into three sorts; those of the first cla A , which constitute at least three-fourths of the whole, are as poor as po ible, and may be thrown away; the scoriæ of the second cla B , which contain some small grains of tin, are sent to the stamps; those of the third cla C , which are last removed from the surface of the bath of tin, are set apart, and re-smelted, as containing a considerable quantity of metal in the form of grain tin. These scoriæ are in small quantity. The stamp slag contains fully 5 per cent. of metallic tin. As soon as the scoriæ are cleared away, the channel is opened which leads to the basin of reception, into which the tin consequently flows out. Here it is left for some time, that the scoriæ which may be still mixed with the metal, may separate, in virtue of the difference of their specific gravities. When the tin has sufficiently settled, it is lifted out with ladles, and poured into cast-iron moulds, in each of which a bit of wood is fixed, to form a hole in the ingot, for the purpose of drawing it out when it becomes cold.
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